diphenyl(4-chlorophenyl)bismuthane

Base Information

Chemical Name:diphenyl(4-chlorophenyl)bismuthane
CAS No.:855253-00-8
Molecular Formula:C₁₈H₁₄BiCl
Molecular Weight:474.743
Hs Code.:

Synonyms:diphenyl(4-chlorophenyl)bismuthane

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Chemical Property of diphenyl(4-chlorophenyl)bismuthane

Chemical Property:

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Technology Process of diphenyl(4-chlorophenyl)bismuthane

There total 4 articles about diphenyl(4-chlorophenyl)bismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 39248-62-9
diphenylbismuthanyl bromide

: 855253-00-8
diphenyl(4-chlorophenyl)bismuthane

Guidance literature:: With p-ClC₆H₄MgX; In diethyl ether; cooling; pouring into H2O, sepn. of ether phase, evapn. of ether;

Reference yield:

: 214141-55-6
(4-chlorophenyl)triphenylbismuthonium tetrafluoroborate

: 855253-00-8
diphenyl(4-chlorophenyl)bismuthane

: 603-33-8
triphenylbismuthane

Guidance literature:: With geraniol; N,N,N',N'-tetramethylguanidine; In dichloromethane; byproducts: geranial, benzene, chlorobenzene; addn. of N,N,N'N'-tetramethylguanidine (0.02 mmol) to mixt. of (4-ClC6H4)Ph3Bi)(BF4) (0.02 mmol), geraniol (0.02 mmol) and CH2Cl2 at 24°C; stirring at the same temp.; GC analysis; concn. under reduced pressure, addn. of CDCl3; monitoring by NNR;
DOI:10.1246/bcsj.81.1621

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 2023-48-5,28719-53-1
triphenylbismuth(V) difluoride

: 855253-00-8
diphenyl(4-chlorophenyl)bismuthane

: 603-33-8
triphenylbismuthane

Guidance literature:: Multi-step reaction with 2 steps

1: water; dichloromethane

2: geraniol; N,N,N',N'-tetramethylguanidine / dichloromethane

With geraniol; N,N,N',N'-tetramethylguanidine; In dichloromethane; water;
DOI:10.1246/bcsj.81.1621