Technology Process of C33H51N5O10SSi2
There total 10 articles about C33H51N5O10SSi2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: trimethylsilyl trifluoromethanesulfonate; DBN / acetonitrile / 21 h / 0 - 65 °C
2.1: sodium methylate / 24 h / 20 °C
3.1: pyridine / 16 h / 20 °C
4.1: pyridine / dichloromethane / 5 h / 20 °C
5.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
6.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
6.2: 1 h / 0 °C
7.1: pyridine / dichloromethane / 3 h / 20 °C
With
pyridine; sodium periodate; trimethylsilyl trifluoromethanesulfonate; DBN; water; sodium methylate; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / 16 h / 20 °C
2.1: pyridine / dichloromethane / 5 h / 20 °C
3.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
4.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
4.2: 1 h / 0 °C
5.1: pyridine / dichloromethane / 3 h / 20 °C
With
pyridine; sodium periodate; water; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;