2,4-dimethoxybenzoyl azide

Base Information

• Chemical Name: 2,4-dimethoxybenzoyl azide
• CAS No.: 90349-41-0
• Molecular Formula: C₉H₉N₃O₃
• Molecular Weight: 207.189

Synonyms:2,4-dimethoxybenzoyl azide

Chemical Property of 2,4-dimethoxybenzoyl azide

Chemical Property:

Purity/Quality:

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Technology Process of 2,4-dimethoxybenzoyl azide

There total 1 articles about 2,4-dimethoxybenzoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dimethoxybenzohydrazide (103956-10-1) → 2,4-dimethoxybenzoyl azide (90349-41-0)

Guidance literature:

With hydrogenchloride; sodium nitrite;

DOI:10.1021/jm00331a021

Reference yield: 49.0%

2,4-dimethoxybenzoyl azide (90349-41-0) + 2,5-dihydro-2,2-dimethoxy-5,5-dimethyl-1,3,4-oxadiazole (138723-90-7) → 1-(2,4-dimethoxyphenyl)-3,3,4,4-tetramethoxyazetidin-2-one

Guidance literature:

In chlorobenzene; for 0.75h; Heating;

DOI:10.1021/ol061101q

Reference yield:

2,4-dimethoxybenzoyl azide (90349-41-0) → 2,4-dimethoxyphenyl isocyanate (84370-87-6)

Guidance literature:

In benzene; Heating;

DOI:10.1016/S0040-4039(99)01392-1

upstream raw materials:

2,4-dimethoxybenzohydrazide

Downstream raw materials:

2,4-dimethoxyphenyl isocyanate

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