Technology Process of (S)-(+)-N-(3-phenyl-pent-4-enyl)-benzamide
There total 3 articles about (S)-(+)-N-(3-phenyl-pent-4-enyl)-benzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: LiAlH4; AlCl3 / tetrahydrofuran / 20 h / Heating
2: 742 mg / triethylamine / diethyl ether / 2 h / cooling
With
lithium aluminium tetrahydride; aluminium trichloride; triethylamine;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jo061664f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 45 percent / P. erythropolis AJ270 containing nitrile hydratase/amidase; potassium phosphate buffer / 24.3 h / 30 °C / pH 7.0
2: LiAlH4; AlCl3 / tetrahydrofuran / 20 h / Heating
3: 742 mg / triethylamine / diethyl ether / 2 h / cooling
With
lithium aluminium tetrahydride; aluminium trichloride; amidase; potassium phosphate buffer; P. erythropolis AJ270 containing nitrile hydratase; triethylamine;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jo061664f
- Guidance literature:
-
With
triethylamine;
In
diethyl ether;
for 2h;
cooling;
DOI:10.1021/jo061664f
