methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

Base Information

Chemical Name:methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate
CAS No.:87580-07-2
Molecular Formula:C₁₁H₁₁Br₂NO₅
Molecular Weight:397.02
Hs Code.:

Synonyms:methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

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Technology Process of methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

There total 11 articles about methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 661453-94-7
3-(2-Benzyloxy-3,5-dibromo-4-methoxy-phenyl)-2-[(Z)-hydroxyimino]-propionic acid methyl ester

: 87580-07-2
methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; acetic acid;

Reference yield: 82.0%

: 184777-86-4
methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

: 87580-07-2
methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

Guidance literature:: With hydrogen; acetic acid; In 1,4-dioxane; at 20 ℃; for 24h; under 760 Torr;
DOI:10.1021/jm051030l

Reference yield: 32.0%

: 87580-09-4,87580-10-7
(5SR,10SR)-methyl 7,9-dibromo-10-hydroxy-8-methoxy-1-oxa-2-azaspiro[4.5]deca-2,6,8-triene-3-carboxylate

: 87580-07-2
methyl 2-hydroxyimino-3-(3,5-dibromo-2-hydroxy-4-methoxyphenyl)propionate

: 50563-30-9
methyl 7,9-dibromo-8-oxo-1-oxa-2-azaspiro<4.5>deca-2,6,9-trien-3-carboxylate

: (+/-)-methyl (1R,2S,6S)-4-bromo-5-oxo-7-oxaspiro[bicyclo[4.1.0]hept-3-ene-2,5'(4'H)isoxazole]-3'-carboxylate

Guidance literature:: (5SR,10SR)-methyl 7,9-dibromo-10-hydroxy-8-methoxy-1-oxa-2-azaspiro[4.5]deca-2,6,8-triene-3-carboxylate; With acetic acid; at 80 ℃;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/j.tetlet.2004.12.084