methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

Base Information

Chemical Name:methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate
CAS No.:184777-86-4
Molecular Formula:C₂₅H₂₃Br₂NO₅
Molecular Weight:577.269
Hs Code.:

Synonyms:methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

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Technology Process of methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

There total 5 articles about methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 35031-38-0
3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

: 184777-86-4
methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

Guidance literature:: In methanol; diethyl ether; at 0 ℃; for 0.166667h;
DOI:10.1016/0040-4020(96)00921-0

Reference yield: 87.0%

: 35031-38-0
3-(2-benzyloxy-3,5-dibromo-4-methoxyphenyl)-2-benzyloxyiminopropanoic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 184777-86-4
methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

Guidance literature:: In methanol; benzene; at 20 ℃; for 0.75h;
DOI:10.1021/jm051030l

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 184777-86-4
methyl 2-benzyloxyimino-3-(2'-benzyloxy-3,5-dibromo-4-methoxyphenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. Ba(OH)2 / dioxane / 1 h / 60 °C

1.2: 75 percent / dioxane / 14 h / 60 °C

2.1: 87 percent / benzene; methanol / 0.75 h / 20 °C

With barium dihydroxide; In 1,4-dioxane; methanol; benzene;
DOI:10.1021/jm051030l