(2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Base Information

Chemical Name:(2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate
CAS No.:1393476-94-2
Molecular Formula:C₂HF₃O₂*C₂₅H₃₄N₄O₆
Molecular Weight:600.592
Hs Code.:

Synonyms:(2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Suppliers and Price of (2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

There total 3 articles about (2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1393477-64-9
tert-butyl (2S)-5-[bis(2-{[(benzyloxy)carbonyl]amino}ethyl)amino]-2-aminopentanoic acid

: 76-05-1
trifluoroacetic acid

: 1393476-94-2
(2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Guidance literature:

Reference yield:

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 1393476-94-2
(2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: dmap; triethylamine / acetonitrile / 2 h / 20 °C

3.1: diisobutylaluminium hydride / diethyl ether; tetrahydrofuran / -78 °C / Inert atmosphere

4.1: acetic acid / dichloromethane / 1 h / 0 °C

4.2: 20 °C

5.1: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C

With hydrogenchloride; dmap; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 129241-89-0
tert-butyl (2S)-2-{bis[(tert-butoxy)carbonyl]amino}-5-oxopentanoate

: 1393476-94-2
(2S)-2-amino-5-[bis(2-{[(benzyloxy)carbonyl] amino}ethyl)amino]pentanoic acid trifluoro acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / dichloromethane / 1 h / 0 °C

1.2: 20 °C

2.1: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C

With hydrogenchloride; acetic acid; In dichloromethane; ethyl acetate;