2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

Base Information

Chemical Name:2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal
CAS No.:123628-95-5
Molecular Formula:C₂₃H₃₄O₂Si₂
Molecular Weight:398.693
Hs Code.:

Synonyms:2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

Chemical Property:

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Technology Process of 2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

There total 5 articles about 2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 201230-82-2
carbon monoxide

: 123628-89-7
(Z)-1-<(1',1'-dimethylethyl)diphenylsilyl>-3-trimethylsilyloxyprop-1-ene

: 123628-95-5
2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

Guidance literature:: With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen; triphenylphosphine; In benzene; at 70 ℃; for 20h; under 20685.9 Torr;

Reference yield:

: 112440-16-1
1-<(1',1'-dimethylethyl)diphenylsilyl>acetylene

: 123628-95-5
2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 2 h, 2.) hexane, THF, RT, 7 h

2: 97 percent / H₂, quinoline / 10percent Pd/CaCO₃ / toluene / 760 Torr / Ambient temperature

3: 88 percent / trimethylsilyl chloride / 1.5 h / 100 °C

4: 72 percent / H₂, carbonylhydridotris(triphenylphosphine)rhodium(I), triphenylphosphine / benzene / 20 h / 70 °C / 20685.9 Torr

With quinoline; carbonylhydridetris(triphenylphosphine)rhodium(I); n-butyllithium; chloro-trimethyl-silane; hydrogen; triphenylphosphine; Lindlar's catalyst; In toluene; benzene;

Reference yield:

: 126741-72-8
1-<(1',1'-dimethylethyl)diphenylsilyl>-3-phenylprop-1-yn-3-ol

: 123628-95-5
2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-trimethylsilyloxypropanal

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / H₂, quinoline / 10percent Pd/CaCO₃ / toluene / 760 Torr / Ambient temperature

2: 88 percent / trimethylsilyl chloride / 1.5 h / 100 °C

3: 72 percent / H₂, carbonylhydridotris(triphenylphosphine)rhodium(I), triphenylphosphine / benzene / 20 h / 70 °C / 20685.9 Torr

With quinoline; carbonylhydridetris(triphenylphosphine)rhodium(I); chloro-trimethyl-silane; hydrogen; triphenylphosphine; Lindlar's catalyst; In toluene; benzene;