N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

Base Information

Chemical Name:N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine
CAS No.:1419075-10-7
Molecular Formula:C₃₀H₃₂N₈O
Molecular Weight:520.637
Hs Code.:

Synonyms:N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

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Chemical Property of N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

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Technology Process of N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

There total 2 articles about N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1419075-09-4
N¹-(prop-2-yn-1-yl)-N¹,N²,N²-tris(pyridin-2-ylmethyl)ethane-1,2-diamine

: 2101-87-3
p-methoxy-phenylazide

: 1419075-10-7
N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 40h; Inert atmosphere;
DOI:10.1021/ic301834x

Reference yield:

: 104170-15-2
N¹,N¹,N²-tris(pyridin-2-ylmethyl)ethane-1,2-diamine

: 1419075-10-7
N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 40 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ic301834x

Reference yield: 55.0%

: sodium hexaflorophosphate

: iron(II) trifluoromethanesulfonate acetonitrile disolvate

: 1419075-10-7
N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine

: [(N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine)Fe](PF₆)₂

Guidance literature:: iron(II) trifluoromethanesulfonate acetonitrile disolvate; N-(1-(4-methoxy-phenyl)-1H-[1,2,3]triazol-4-ylmethyl)-N,N′,N′-tris(pyridin-2-ylmethyl)-ethane-1,2-diamine; In ethanol; for 0.5h; Inert atmosphere; Glovebox;

sodium hexaflorophosphate; In ethanol; Inert atmosphere; Glovebox;
DOI:10.1021/ic301834x