1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

Base Information

Chemical Name:1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene
CAS No.:51501-79-2
Molecular Formula:C₂₆H₂₂O₂
Molecular Weight:366.459
Hs Code.:

Synonyms:1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

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Chemical Property of 1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

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Technology Process of 1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

There total 7 articles about 1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 92-86-4
4-(4-bromophenyl)bromobenzene

: 5720-07-0
4-methoxyphenylboronic acid

: 51501-79-2
1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

Guidance literature:: With cesium fluoride; tetrakis-(triphenylphosphino)-palladium⁽⁰⁾; In tetrahydrofuran; for 50h; Heating;
DOI:10.1055/s-2007-965891

Reference yield: 71.0%

: sodium trihydroxy(4-methoxyphenyl)borate

: 34176-08-4
sodium 4-bromobenzenesulfinate

: 51501-79-2
1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

Guidance literature:: sodium 4-bromobenzenesulfinate; With copper(I) oxide; oxygen; palladium dichloride; In water; at 100 ℃; for 30h; Sealed tube;

sodium trihydroxy(4-methoxyphenyl)borate; With tetrabutylammomium bromide; In water; at 100 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c2gc36550b

Reference yield: 51.0%

: 1679-18-1
4-Chlorophenylboronic acid

: 5720-07-0
4-methoxyphenylboronic acid

: 13331-27-6
m-nitrobenzene boronic acid

: 51501-79-2
1,4'''-dimethoxy-4,1':4',1'':4'',1'''-quaterphenylene

: 4''-methoxy-3-nitro-1,1':4',1''-terphenyl

: C₁₉H₁₅ClO

Guidance literature:: 4-Chlorophenylboronic acid; m-nitrobenzene boronic acid; With potassium carbonate; In water; acetonitrile; at 70 ℃; for 48h; Schlenk technique;

4-methoxyphenylboronic acid; With XPhos; In water; acetonitrile; at 70 ℃; for 24h; Schlenk technique;
DOI:10.1002/asia.201800358