2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

Base Information

Chemical Name:2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester
CAS No.:292148-40-4
Molecular Formula:C₁₇H₂₀O₅
Molecular Weight:304.343
Hs Code.:

Synonyms:2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

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Chemical Property of 2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

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Technology Process of 2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

There total 3 articles about 2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 79-41-4,25087-26-7,50867-57-7
poly(methacrylic acid)

: 183624-93-3
(3R,3aR,6R,6aR)-6-benzyloxy-2,3,3a,5,6,6a-hexahydrofuro[3,2-b]furan-3-ol

: 292148-40-4
2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃;
DOI:10.1021/jo0155153

Reference yield:

: 100-39-0
benzyl bromide

: 292148-40-4
2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / NaH; Bu₄NI / dimethylformamide / 20 °C

2: 70 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0155153

Reference yield:

: 641-74-7
1,4:3,6-dianhydro-D-mannitol

: 292148-40-4
2-Methyl-acrylic acid (3R,3aR,6R,6aR)-6-benzyloxy-hexahydro-furo[3,2-b]furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / NaH; Bu₄NI / dimethylformamide / 20 °C

2: 70 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0155153