1H-Pyrrole-2-carboxaldehyde, 5-(methoxymethyl)-1-methyl- (9CI)

Base Information

• Chemical Name: 1H-Pyrrole-2-carboxaldehyde, 5-(methoxymethyl)-1-methyl- (9CI)
• CAS No.: 88065-99-0
• Molecular Formula: C₈H₁₁NO₂
• Molecular Weight: 153.181
• Hs Code.: 2933990090
• Mol file: 88065-99-0.mol

Synonyms:1H-Pyrrole-2-carboxaldehyde, 5-(methoxymethyl)-1-methyl- (9CI)

Chemical Property of 1H-Pyrrole-2-carboxaldehyde, 5-(methoxymethyl)-1-methyl- (9CI)

Chemical Property:

• PSA: 31.23000
• LogP: 0.98400

Purity/Quality:

5-(methoxymethyl)-1-methyl-1H-Pyrrole-2-carboxaldehyde 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrole-2-carboxaldehyde, 5-(methoxymethyl)-1-methyl- (9CI)

There total 6 articles about 1H-Pyrrole-2-carboxaldehyde, 5-(methoxymethyl)-1-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

sodium methylate (124-41-4) + (S)-Methyl-phosphonothioic acid O-((2R,3R,4R,5S,6R)-4,5-dimethoxy-6-methoxymethyl-3-methylamino-tetrahydro-pyran-2-yl) ester O-ethyl ester (88065-90-1) → 1-methyl-5-methoxymethylpyrrole-2-carbaldehyde (88065-99-0) + (S)-(-)-O-ethyl O-methyl methylphosphonothioate (88066-00-6)

Guidance literature:

In methanol; for 48h; Ambient temperature;

Reference yield: 55.0%

sodium ethanolate (141-52-6) + (S)-Methyl-phosphonothioic acid O-((2S,3R,4R,5S,6R)-4,5-dimethoxy-6-methoxymethyl-3-methylamino-tetrahydro-pyran-2-yl) ester O-ethyl ester (88065-92-3) → O,O-diethyl methanephosphonothionate (6996-81-2) + 1-methyl-5-methoxymethylpyrrole-2-carbaldehyde (88065-99-0) + C3H8O2PS(1-)*Na(1+) (88065-98-9) + ethyl 2-deoxy-2-methylamino-3,4,5-tri-O-methyl-β-D-glucopyranoside (88065-97-8)

Guidance literature:

In ethanol; Further byproducts given;

Reference yield: 45.0%

2-deoxy-2-methylamino-3,4,6-tri-O-methyl-α,β-D-glucose hydrochloride (36757-12-7) → 1-methyl-5-methoxymethylpyrrole-2-carbaldehyde (88065-99-0)

Guidance literature:

With sodium methylate; In methanol; at 25 ℃; for 48h;

upstream raw materials:

sodium methylate

(S)-Methyl-phosphonothioic acid O-((2R,3R,4R,5S,6R)-4,5-dimethoxy-6-methoxymethyl-3-methylamino-tetrahydro-pyran-2-yl) ester O-ethyl ester

sodium ethanolate

(S)-Methyl-phosphonothioic acid O-((2S,3R,4R,5S,6R)-4,5-dimethoxy-6-methoxymethyl-3-methylamino-tetrahydro-pyran-2-yl) ester O-ethyl ester

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