phenoxysubphthalocyaninatoboron

Base Information

• Chemical Name: phenoxysubphthalocyaninatoboron
• CAS No.: 182575-04-8
• Molecular Formula: C₃₀H₁₇BN₆O
• Molecular Weight: 488.316
• Mol file: 182575-04-8.mol

Synonyms:phenoxysubphthalocyaninatoboron

Chemical Property of phenoxysubphthalocyaninatoboron

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of phenoxysubphthalocyaninatoboron

There total 18 articles about phenoxysubphthalocyaninatoboron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

subphthalocyanine (36530-06-0) + phenol (108-95-2,27073-41-2) → phenoxysubphthalocyaninatoboron (182575-04-8)

Guidance literature:

In toluene; at 110 ℃; Inert atmosphere;

DOI:10.1039/b922199a

Reference yield: 89.0%

phenyltrimethylsilyl ether (1529-17-5) + subphthalocyanine (36530-06-0) → phenoxysubphthalocyaninatoboron (182575-04-8)

Guidance literature:

In toluene; for 9h; Reflux;

DOI:10.1021/acs.orglett.5b02213

Reference yield: 48.0%

(OTf)B(NC8H4(N))3 + methoxybenzene (100-66-3) → phenoxysubphthalocyaninatoboron (182575-04-8)

Guidance literature:

With lithium hexamethyldisilazane; In hexane; benzene; at 40 ℃; for 65h; Schlenk technique;

DOI:10.1021/acs.organomet.6b00754

upstream raw materials:

bromo-[7,12:14,19-diimino-21,5-nitrilo-5H-tribenzo[c,h,m][1,6,11]triazacyclopentadecinato-(2)-κN22,κN23,κN24]-boron(III)

phenol

boron tribromide

phthalonitrile