C₂₂H₂₈N₂O₅

Base Information

Chemical Name:C₂₂H₂₈N₂O₅
CAS No.:1333114-71-8
Molecular Formula:C₂₂H₂₈N₂O₅
Molecular Weight:400.475
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₂H₂₈N₂O₅

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Chemical Property of C₂₂H₂₈N₂O₅

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Technology Process of C₂₂H₂₈N₂O₅

There total 3 articles about C₂₂H₂₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1333114-70-7
C₂₀H₂₅BrN₂O₃

: 1333114-71-8
C₂₂H₂₈N₂O₅

Guidance literature:: With triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; at 120 ℃; for 30h; under 7500.75 Torr;

Reference yield:

: 38749-79-0
3-bromo-2-picoline

: 1333114-71-8
C₂₂H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

2.2: 16 h / 20 °C

3.1: triethylamine / 1,3-bis-(diphenylphosphino)propane; palladium diacetate / 30 h / 120 °C / 7500.75 Torr

With N-Bromosuccinimide; sodium hydride; triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide;

Reference yield:

: 754131-60-7
3-bromo-2-(bromomethyl)pyridine

: 1333114-71-8
C₂₂H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

1.2: 16 h / 20 °C

2.1: triethylamine / 1,3-bis-(diphenylphosphino)propane; palladium diacetate / 30 h / 120 °C / 7500.75 Torr

With sodium hydride; triethylamine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; In N,N-dimethyl-formamide;