(2-diethylphosphinoethyl)triphenylstannane

Base Information

Chemical Name:(2-diethylphosphinoethyl)triphenylstannane
CAS No.:75271-67-9
Molecular Formula:C₂₄H₂₉PSn
Molecular Weight:467.178
Hs Code.:

Synonyms:(2-diethylphosphinoethyl)triphenylstannane

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Chemical Property of (2-diethylphosphinoethyl)triphenylstannane

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Technology Process of (2-diethylphosphinoethyl)triphenylstannane

There total 1 articles about (2-diethylphosphinoethyl)triphenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 13652-21-6
diethylvinyl phosphine

: 892-20-6
triphenylstannane

: 75271-67-9
(2-diethylphosphinoethyl)triphenylstannane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In neat (no solvent); under protective gas addn. of AIBN to the mixt. of (C6H5)3SnH and (CH3CH2)2PCHCH2 without solvent slowly heating to 60-70°C, then 6-7 h at 70-90°C meanwhile addn. of the rest of AIBN; vac. distn., elem. anal.;

Reference yield: 75.1%

: 75271-67-9
(2-diethylphosphinoethyl)triphenylstannane

: sodium triphenylstannide

Guidance literature:: With sodium; ammonium bromide; In diethyl ether; ammonia; byproducts: NaBr, (C2H5)3P; under protective gas prepd. the suspn. of (C6H5)3SnCH2CH2P(C2H5)2 with ether in NH3 liq. addn. of Na at -50°C, at end of react. the soln. blue-coloured, addn. of NH4Br, discolouration, evapn. of NH3, addn. ofether, pptn.; addn. of THF, filtration of NaBr, concd. of soln., addn. of ether, pptn., filtration, washing with ether, elem. anal.;