dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

Base Information

Chemical Name:dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester
CAS No.:899794-54-8
Molecular Formula:C₁₉H₂₆O₅S₂
Molecular Weight:398.544
Hs Code.:

Synonyms:dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

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Chemical Property of dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

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Technology Process of dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

There total 5 articles about dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 22515-82-8
1-pentene-3-one ethylene acetal

: 93624-01-2
O-ethyl S-2-(4-methoxyphenyl)-2-oxoethyl carbonodithioate

: 899794-54-8
dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

Guidance literature:: With 2,6-dimethylpyridine; dilauryl peroxide; In cyclohexane; Heating;
DOI:10.1055/s-2006-926464

Reference yield:

: 899794-48-0
2-ethyl-2-[2-(toluene-4-sulfonyl)-ethyl]-[1,3]dioxolane

: 899794-54-8
dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / dimethylethylene urea; t-BuOK / Heating

2: 69 percent / 2,6-lutidine; dilauroyl peroxide / cyclohexane / Heating

With 2,6-dimethylpyridine; dimethyl-ethylene urea; dilauryl peroxide; potassium tert-butylate; In cyclohexane;
DOI:10.1055/s-2006-926464

Reference yield:

: 32830-97-0
1-chloro-3-pentanone

: 899794-54-8
dithiocarbonic acid O-ethyl ester S-[4-(4-methoxyphenyl)-1-(2-ethyl[1,3]dioxolan-2-yl)-4-oxobutyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / ethanol / 4 h / Heating

2: 85 percent / p-TsOH / toluene / 8 h / Heating

3: 85 percent / dimethylethylene urea; t-BuOK / Heating

4: 69 percent / 2,6-lutidine; dilauroyl peroxide / cyclohexane / Heating

With 2,6-dimethylpyridine; dimethyl-ethylene urea; dilauryl peroxide; potassium tert-butylate; toluene-4-sulfonic acid; In ethanol; cyclohexane; toluene;
DOI:10.1055/s-2006-926464