tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Base Information

Chemical Name:tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate
CAS No.:1207984-86-8
Molecular Formula:C₂₅H₂₆ClN₅O₄
Molecular Weight:495.966
Hs Code.:

Synonyms:tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

There total 8 articles about tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1207984-80-2
10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

: 1207984-86-8
tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 2h;

Reference yield:

: 95-74-9,827571-80-2
3-chloro-p-toluidine

: 1207984-86-8
tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; triethylamine / ethyl acetate / 6 h / 0 - 20 °C

2.1: nitric acid; acetic anhydride / acetic acid / 5 h / -10 - 20 °C

3.1: methanol; sodium methylate / 5 h / 20 °C

4.1: ammonium chloride / ethanol / Reflux; Inert atmosphere

5.1: sodium tetrahydroborate / ethanol / 12 h / Reflux

5.2: 0 - 20 °C

6.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

7.1: sulfuric acid; periodic acid / water / 0 - 20 °C

7.2: pH 3.8 - 3.9

8.1: acetic acid / ethanol / 20 - 40 °C

8.2: 2 h / 20 °C

9.1: triethylamine / methanol / 2 h / 20 °C

With methanol; dmap; boron trioxide; sodium tetrahydroborate; sulfuric acid; nitric acid; sodium methylate; acetic anhydride; ammonium chloride; acetic acid; periodic acid; triethylamine; In methanol; ethanol; water; acetic acid; ethyl acetate;

Reference yield:

: 1207983-26-3
(2R,3S,4S)-5-(2-amino-5-chloro-4-methylphenylamino)pentane-1,2,3,4-tetraol

: 1207984-86-8
tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

2.1: sulfuric acid; periodic acid / water / 0 - 20 °C

2.2: pH 3.8 - 3.9

3.1: acetic acid / ethanol / 20 - 40 °C

3.2: 2 h / 20 °C

4.1: triethylamine / methanol / 2 h / 20 °C

With boron trioxide; sulfuric acid; acetic acid; periodic acid; triethylamine; In methanol; ethanol; water;