((pentafluorosulfanyl)imino)chlorofluorosulfane

Base Information

Chemical Name:((pentafluorosulfanyl)imino)chlorofluorosulfane
CAS No.:80997-19-9
Molecular Formula:ClF₆NS₂
Molecular Weight:227.582
Hs Code.:

Synonyms:((pentafluorosulfanyl)imino)chlorofluorosulfane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((pentafluorosulfanyl)imino)chlorofluorosulfane

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Technology Process of ((pentafluorosulfanyl)imino)chlorofluorosulfane

There total 2 articles about ((pentafluorosulfanyl)imino)chlorofluorosulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 13774-70-4
((pentafluorosulfanyl)imino)difluorosulfane

: 7647-18-9
antimonypentachloride

: 25502-15-2
SF₅N=SCl₂

: 80997-19-9
((pentafluorosulfanyl)imino)chlorofluorosulfane

: 7783-70-2
antimony pentafluoride

Guidance literature:: sulfane was condesed on SbCl5 at -196°C, heated at 100°C to initiate the reaction; fractionation through a series of traps at -6, -45, -78, -112 and -196°C in vac., a -45°C trap contained the product;

Reference yield: 9.6%

: 7719-09-7
thionyl chloride

: 15930-75-3
thiazyl trifluoride

: 7664-39-3,12381-92-9,32057-09-3,74835-82-8
hydrogen fluoride

: 25502-15-2
SF₅N=SCl₂

: 80997-19-9
((pentafluorosulfanyl)imino)chlorofluorosulfane

: 7783-42-8
thionyl fluoride

Guidance literature:: HF and NSF3 were condesed in Kel-F reactor at -196°C, allowed toreact at room temp. overnight, SOCl2 added, reacted at room temp. for 2weeks and volatile products were condensed into a NaF scrubber; fractionation through a series of traps at -10, -78, and -196°C in vac., a -78°C trap contained the product, distillation;

upstream raw materials:

((pentafluorosulfanyl)imino)difluorosulfane

antimonypentachloride

thionyl chloride

thiazyl trifluoride

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