(±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

Base Information

Chemical Name:(±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine
CAS No.:1395280-10-0
Molecular Formula:C₁₅H₂₀N₂O₃Si
Molecular Weight:304.421
Hs Code.:

Synonyms:(±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

Chemical Property:

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Technology Process of (±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

There total 1 articles about (±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 1187055-95-3
(±)-5-methyl-3-(3-nitropyridin-4-yl)cyclohex-2-enone

: 1395280-10-0
(±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

Reference yield:

: 1395280-10-0
(±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

: 33797-51-2
eschenmoser's salt

: 1395280-12-2
(±)-6-((dimethylamino)methyl)-5-methyl-3-(3-nitropyridin-4-yl)cyclohex-2-enone

Guidance literature:: (±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine; eschenmoser's salt; In dichloromethane; at 0 - 20 ℃; for 19h;

With hydrogenchloride; In dichloromethane; water; at 0 ℃; for 0.333333h;

With sodium hydroxide; In dichloromethane; water; at 0 ℃; for 1h;

Reference yield:

: 1395280-10-0
(±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine

: 33797-51-2
eschenmoser's salt

: (5S)-6-[(dimethylamino)methyl]-5-methyl-3-(3-nitropyridin-4-yl)cyclohex-2-en-1-one

Guidance literature:: (±)-4-(5-methyl-3-(trimethylsilyloxy)cyclohexa-1,3-dienyl)-3-nitropyridine; eschenmoser's salt; In dichloromethane; at 0 - 30 ℃; for 18h;

With hydrogenchloride; water; In dichloromethane; at 0 ℃; for 0.333333h;