(E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate

Base Information

• Chemical Name: (E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate
• CAS No.: 854737-57-8
• Molecular Formula: C₂₂H₃₈O₄Si₂
• Molecular Weight: 422.712

Synonyms:(E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate

Chemical Property of (E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate

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Technology Process of (E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate

There total 2 articles about (E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid (1135-24-6,537-98-4) + tert-butyldimethylsilyl chloride (18162-48-6) → (E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate (854737-57-8)

Guidance literature:

With 1H-imidazole; dmap; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2005.03.074

Reference yield: 13.0%

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid (1135-24-6,537-98-4) + tert-butyldimethylsilyl chloride (18162-48-6) → (E)‐3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylic acid (854737-54-5) + (E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate (854737-57-8)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/acs.jnatprod.8b00439

Reference yield: 100.0%

(E)‐tert‐butyldimethylsilyl3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylate (854737-57-8) → (E)‐3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylic acid (854737-54-5)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.5h;

DOI:10.1021/acs.jnatprod.8b00439

upstream raw materials:

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

tert-butyldimethylsilyl chloride

Downstream raw materials:

(E)‐3‐(4‐((tert‐butyldimethylsilyl)oxy)‐3‐methoxyphenyl)acrylic acid

3-[4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-acrylic acid 3-[4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-2-oxo-propyl ester

3-[4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-phenyl]-acrylic acid 3-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-oxo-propyl ester

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