2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

Base Information

Chemical Name:2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone
CAS No.:1257079-45-0
Molecular Formula:C₃₆H₂₉N₃O₆
Molecular Weight:599.643
Hs Code.:

Synonyms:2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

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Chemical Property of 2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

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Technology Process of 2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

There total 4 articles about 2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 41572-86-5
N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide

: 1257079-45-0
2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

Guidance literature:: With nitric acid; In dichloromethane; at 25 ℃;
DOI:10.1177/1747519819886502

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1257079-45-0
2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1-methyl-pyrrolidin-2-one

2: ammonium cerium (IV) nitrate; nitric acid / dichloromethane / 2 h / 25 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; nitric acid; acetic acid; In 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1016/j.dyepig.2011.06.023

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 1257079-45-0
2,9-dicyclohexyl-5-nitroanthra[2,1,9-def:6,5,10-d′e′f′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1-methyl-pyrrolidin-2-one

2: ammonium cerium (IV) nitrate; nitric acid / dichloromethane / 2 h / 25 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; nitric acid; acetic acid; In 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1016/j.dyepig.2011.06.023