(+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

Base Information

Chemical Name:(+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate
CAS No.:1315128-25-6
Molecular Formula:C₃₂H₃₁NO₃
Molecular Weight:477.603
Hs Code.:

Synonyms:(+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

Chemical Property:

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Technology Process of (+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

There total 3 articles about (+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1315179-34-0
(-)-phenylmethyl formyl((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

: 1315128-25-6
(+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 2h;
DOI:10.1002/chem.201100649

Reference yield:

: C₂₆H₂₆O₄

: 1315128-25-6
(+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / tetrahydrofuran / 2.5 h / 50 °C / Inert atmosphere

2: potassium hydroxide / methanol / 2 h / 20 °C

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201100649

Reference yield:

: 69261-49-0
benzyl formylcarbamate

: 1315128-25-6
(+)-phenylmethyl ((1S)-1-{2-[(triphenylmethyl)oxy]ethyl}prop-2-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / tetrahydrofuran / 2.5 h / 50 °C / Inert atmosphere

2: potassium hydroxide / methanol / 2 h / 20 °C

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201100649