2-phenylethynyl N-benzylidene glycinate

Base Information

Chemical Name:2-phenylethynyl N-benzylidene glycinate
CAS No.:944925-90-0
Molecular Formula:C₁₈H₁₅NO₂
Molecular Weight:277.323
Hs Code.:

Synonyms:2-phenylethynyl N-benzylidene glycinate

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Chemical Property of 2-phenylethynyl N-benzylidene glycinate

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Technology Process of 2-phenylethynyl N-benzylidene glycinate

There total 1 articles about 2-phenylethynyl N-benzylidene glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59046-72-9
o-(phenylethynyl)benzaldehyde

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 944925-90-0
2-phenylethynyl N-benzylidene glycinate

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; Molecular sieve;
DOI:10.1021/ol3026507

Reference yield: 78.0%

: 67-56-1
methanol

: 944925-90-0
2-phenylethynyl N-benzylidene glycinate

: 122778-92-1
2-(2-Hydroxy-5-methylphenyl)-1-phenylethin

: methyl 9-methoxy-9-methyl-12-oxo-6-phenyl-12a-(phenylethynyl)-8,8a,9,12,12a,12b-hexahydroisoindolo[1,2-a]isoquinoline-8-carboxylate

Guidance literature:: methanol; 2-(2-Hydroxy-5-methylphenyl)-1-phenylethin; With iodosylbenzene; at 25 ℃; for 0.0833333h; Schlenk technique; Inert atmosphere;

2-phenylethynyl N-benzylidene glycinate; With silver fluoride; In 1,2-dichloro-ethane; at 25 ℃; for 10h; Reagent/catalyst; Solvent; diastereoselective reaction; Catalytic behavior; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02329

Reference yield: 72.0%

: 67-56-1
methanol

: 944925-90-0
2-phenylethynyl N-benzylidene glycinate

: C₁₅H₁₁BrO

: methyl 12a-((4-bromophenyl)ethynyl)-9-methoxy-9-methyl-12-oxo-6-phenyl-8,8a,9,12,12a,12b-hexahydroisoindolo[1,2-a]isoquinoline-8-carboxylate

Guidance literature:: methanol; C₁₅H₁₁BrO; With iodosylbenzene; at 25 ℃; for 0.0833333h; Schlenk technique; Inert atmosphere;

2-phenylethynyl N-benzylidene glycinate; With silver fluoride; In 1,2-dichloro-ethane; at 25 ℃; for 10h; diastereoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02329