1,2-diphenyldiazoethane

Base Information

Chemical Name:1,2-diphenyldiazoethane
CAS No.:40145-79-7
Molecular Formula:C₁₄H₁₂N₂
Molecular Weight:208.263
Hs Code.:

Synonyms:1,2-diphenyldiazoethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-diphenyldiazoethane

Chemical Property:

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Technology Process of 1,2-diphenyldiazoethane

There total 4 articles about 1,2-diphenyldiazoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5171-96-0
(1,2-diphenylethylidene)hydrazine

: 40145-79-7
1,2-diphenyldiazoethane

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - -55 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.orglett.5b02370

Reference yield:

: 82222-56-8
Deoxybenzoin 2,4,6-triisopropylbenzenesulphonyl hydrazone

: 40145-79-7
1,2-diphenyldiazoethane

Guidance literature:: With potassium hydroxide; In methanol; for 0.166667h; Heating;
DOI:10.1055/s-1982-29821

Reference yield:

: 451-40-1
phenyl benzyl ketone

: 40145-79-7
1,2-diphenyldiazoethane

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / conc. HCl / methanol / 1 h / Ambient temperature

2: KOH / methanol / 0.17 h / Heating

With hydrogenchloride; potassium hydroxide; In methanol;
DOI:10.1055/s-1982-29821