1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

Base Information

Chemical Name:1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone
CAS No.:1529853-61-9
Molecular Formula:C₂₅H₂₇N₃O
Molecular Weight:385.509
Hs Code.:

Synonyms:1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

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Chemical Property of 1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

Chemical Property:

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Technology Process of 1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

There total 4 articles about 1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1175004-74-6
1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde

: 100-63-0
phenylhydrazine

: 1529853-61-9
1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

Guidance literature:: In isopropyl alcohol; for 1h; Reflux;

Reference yield:

: 3297-78-7
acetic acid 1-phenyl-1,2,3,4-tetrahydro-quinolin-3-yl ester

: 1529853-61-9
1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate

2: potassium hydroxide / methanol; water / 0.58 h / Reflux

3: potassium hydroxide; sodium sulfate / N,N-dimethyl-formamide / 60 - 65 °C

4: isopropyl alcohol / 3 h / 85 °C

With sodium sulfate; potassium hydroxide; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol; 1: |Vilsmeier-Haack Formylation;
DOI:10.1016/j.dyepig.2014.01.010

Reference yield:

: 934420-64-1
3-acetyl-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde

: 1529853-61-9
1-phenyl-3-propoxy-1,2,3,4-tetrahydroquinoline-6-carbaldehyde N-phenylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / methanol; water / 0.58 h / Reflux

2: potassium hydroxide; sodium sulfate / N,N-dimethyl-formamide / 60 - 65 °C

3: isopropyl alcohol / 3 h / 85 °C

With sodium sulfate; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.dyepig.2014.01.010