Technology Process of C12H16O3
There total 6 articles about C12H16O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 4h;
stereoselective reaction;
DOI:10.1016/j.tetlet.2013.07.115
- Guidance literature:
-
Multi-step reaction with 4 steps
1: titanium(IV) isopropylate / toluene / 12 h / 100 °C
2: zinc(II) chloride / diethyl ether / -78 - 25 °C
3: potassium hydroxide; water / methanol / Reflux
4: potassium carbonate / N,N-dimethyl-formamide / 4 h / 25 °C
With
titanium(IV) isopropylate; water; potassium carbonate; potassium hydroxide; zinc(II) chloride;
In
methanol; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2013.07.115
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aluminum (III) chloride / 1,2-dichloro-ethane / 4 h / 0 - 30 °C
2: titanium(IV) isopropylate / toluene / 12 h / 100 °C
3: zinc(II) chloride / diethyl ether / -78 - 25 °C
4: potassium hydroxide; water / methanol / Reflux
5: potassium carbonate / N,N-dimethyl-formamide / 4 h / 25 °C
With
titanium(IV) isopropylate; aluminum (III) chloride; water; potassium carbonate; potassium hydroxide; zinc(II) chloride;
In
methanol; diethyl ether; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
1: |Friedel-Crafts Acylation;
DOI:10.1016/j.tetlet.2013.07.115
