phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

Base Information

Chemical Name:phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester
CAS No.:618068-84-1
Molecular Formula:C₂₁H₂₄O₄
Molecular Weight:340.419
Hs Code.:

Synonyms:phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

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Chemical Property of phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

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Technology Process of phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

There total 3 articles about phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 103-82-2
phenylacetic acid

: 618068-80-7
1-[2-(2-methyl-[1,3]dioxolan-2-yl)phenyl]propan-2-ol

: 618068-84-1
phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/ol035782q

Reference yield:

: 50777-64-5
2-(2-bromophenyl)-2-methyl-1,3-dioxolane

: 618068-84-1
phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Li / diethyl ether / 2 h

1.2: 64 percent / diethyl ether / 2 h

2.1: 53 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂

With dmap; lithium; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1021/ol035782q

Reference yield:

: 2142-69-0
2-bromophenyl methyl ketone

: 618068-84-1
phenylacetic acid 1-methyl-2-[2-(2-methyl-[1,3]dioxolan-2-yl)-phenyl]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: p-TsOH

2.1: Li / diethyl ether / 2 h

2.2: 64 percent / diethyl ether / 2 h

3.1: 53 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂

With dmap; lithium; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1021/ol035782q