tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate

Base Information

Chemical Name:tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate
CAS No.:82112-30-9
Molecular Formula:C15H34 O3 Si2
Molecular Weight:0
Hs Code.:
Mol file:82112-30-9.mol

Synonyms:tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate

Suppliers and Price of tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate

Chemical Property:

Melting Point:159 - 162 °C
PSA：35.53000
LogP:4.94670

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate

There total 2 articles about tert-Butyl(dimethyl)silyl 3-([tert-butyl(dimethyl)silyl]oxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 77377-52-7
N-methyl-N-tert-butyldimethylsilyl-1,1,1-trifluoroacetamide

: 503-66-2
3-hydroxypropionic acid

: 82112-30-9
C₁₅H₃₄O₃Si₂

Guidance literature:: With tert-butyldimethylsilyl chloride; In acetonitrile; for 0.0833333h; Ambient temperature; other silylating agent;
DOI:10.1021/jo00138a032

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 82112-30-9
C₁₅H₃₄O₃Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) benzene, acetonitrile, 4 deg C, 4 h, 2.) 2 h

2: 100 percent / 1percent tert-butyldimethylsilyl chloride (TBDMSCl) / acetonitrile / 0.08 h / Ambient temperature; other silylating agent

With sodium hydride; tert-butyldimethylsilyl chloride; In acetonitrile;
DOI:10.1021/jo00138a032