[Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

Base Information

Chemical Name:[Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2
CAS No.:172301-92-7
Molecular Formula:C₂₆H₃₆Br₂Cu₂N₆O₂
Molecular Weight:751.511
Hs Code.:

Synonyms:[Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

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Chemical Property of [Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

Chemical Property:

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Technology Process of [Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

There total 3 articles about [Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 637015-42-0
((C₆H₅)3P)Au(CCC(CH₂)CH₃)

: C₆H₅CH₂OC₆H₄C₁₂H₆N₂C₆H₄OC(O)(CH₂)4C₃H₅S₂

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl

: [Pt3(μ-CNXyl)2(μ-CO)(CNXyl)(PCy3)2]

: 7647-15-6
sodium bromide

: C₆H₅CH₂OC₆H₄C₁₂H₄N₂(CH₃)2C₆H₄OC(O)(CH₂)4C₃H₅S₂

: 1179-06-2
1,4-Bis(diphenylphosphino)benzene

: 2P(C₆H₅)4⁽¹⁺⁾*Ir₆^(2-)*15CO=(P(C₆H₅)4)2{Ir₆(CO)15}

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 172301-92-7
[Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

: Ir₆*16(CO)=Ir₆(CO)16

: [(1,4-(CuPPh2)2C6H4)(Pt3(μ2-CO)(μ2-CNXyl)2(CNXyl)(PCy3)2)2][PF6]2

Guidance literature:: In dichloromethane; Ar-atmosphere; stoich. amts.; dropwise addn. of mixt. of Cu-complex and phosphine (in CH2Cl2 or THF, not specified) to Pt-complex, stirring for 30 min; concn., pptn. on hexane addn.; elem. anal.;

Reference yield:

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 637015-42-0
((C₆H₅)3P)Au(CCC(CH₂)CH₃)

: C₆H₅CH₂OC₆H₄C₁₂H₆N₂C₆H₄OC(O)(CH₂)4C₃H₅S₂

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl

: [Pt3(μ-CNXyl)2(μ-CO)(CNXyl)(PCy3)2]

: 7647-15-6
sodium bromide

: C₆H₅CH₂OC₆H₄C₁₂H₄N₂(CH₃)2C₆H₄OC(O)(CH₂)4C₃H₅S₂

: 1179-06-2
1,4-Bis(diphenylphosphino)benzene

: 2P(C₆H₅)4⁽¹⁺⁾*Ir₆^(2-)*15CO=(P(C₆H₅)4)2{Ir₆(CO)15}

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 172301-92-7
[Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

: Ir₆*16(CO)=Ir₆(CO)16

: [(1,4-(CuPPh2)2C6H4)(Pt3(μ2-CO)(μ2-CNXyl)2(CNXyl)(PCy3)2)2][PF6]2

: [η2-((triphenylphosphine)Au(CCC(CH2)Me))2Cu]PF6*0.5(dichloromethane)

Guidance literature:: In nitromethane-d3; (inert atm.); reaction of copper compd. with 2 equiv. of bipyridine deriv. in nitromethane-d3 at room temp., addn. of 4 equiv. of ruthenium compd.;
DOI:10.1021/ic7018428

Reference yield:

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 637015-42-0
((C₆H₅)3P)Au(CCC(CH₂)CH₃)

: C₆H₅CH₂OC₆H₄C₁₂H₆N₂C₆H₄OC(O)(CH₂)4C₃H₅S₂

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl

: [Pt3(μ-CNXyl)2(μ-CO)(CNXyl)(PCy3)2]

: 7647-15-6
sodium bromide

: C₆H₅CH₂OC₆H₄C₁₂H₄N₂(CH₃)2C₆H₄OC(O)(CH₂)4C₃H₅S₂

: 1179-06-2
1,4-Bis(diphenylphosphino)benzene

: 2P(C₆H₅)4⁽¹⁺⁾*Ir₆^(2-)*15CO=(P(C₆H₅)4)2{Ir₆(CO)15}

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 172301-92-7
[Cu(μ-Br)(2-(6'-methyl-2'-pyridyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazolyl-1-oxyl)]2

: Ir₆*16(CO)=Ir₆(CO)16

: [(1,4-(CuPPh2)2C6H4)(Pt3(μ2-CO)(μ2-CNXyl)2(CNXyl)(PCy3)2)2][PF6]2

: [η2-((triphenylphosphine)Au(CCC(CH2)Me))2Cu]PF6*0.5(dichloromethane)

: Ir₆(CO)15(Cu(NCCH₃))2

Guidance literature:: In dichloromethane; (C5H4N)2 added to a soln. of Cu complex and C12H6N2(C6H2(CH3)3)2; solvent-removed; elem. anal.;
DOI:10.1021/ic900657w