oxo(propylamino)acetic acid

Base Information

• Chemical Name: oxo(propylamino)acetic acid
• CAS No.: 81682-53-3
• Molecular Formula: C5H9 N O3
• Molecular Weight: 131.131
• Hs Code.: 2924199090
• Mol file: 81682-53-3.mol

Synonyms:Aceticacid, oxo(propylamino)- (9CI); N-Propyloxamic acid

Chemical Property of oxo(propylamino)acetic acid

Chemical Property:

• Refractive Index: 1.456
• PSA: 66.40000
• Density: 1.174g/cm³
• LogP: -0.01190
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

Oxo(propylamino)acetic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of oxo(propylamino)acetic acid

There total 5 articles about oxo(propylamino)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

propylamine (107-10-8,42939-71-9) + L-threo-2,3-hexodiulosono-1,4-lactone (490-83-5,5959-82-0,7723-73-1,19192-77-9,33124-69-5,34481-26-0,61586-47-8,106033-44-7,111399-75-8) → oxalic acid monopropylamide (81682-53-3)

Guidance literature:

With phosphate buffer; at 100 ℃; for 2h;

DOI:10.1021/jf9601426

Reference yield: 10.0%

propylamine (107-10-8,42939-71-9) + oxalyl dichloride (79-37-8) → oxalic acid monopropylamide (81682-53-3)

Guidance literature:

at -17 ℃; for 3h;

DOI:10.1021/jf9601426

Reference yield:

ethyl 2-(propylamino)-2-oxoacetate (20943-65-1) → oxalic acid monopropylamide (81682-53-3)

Guidance literature:

With potassium hydroxide; In ethanol;

DOI:10.1016/0584-8539(96)01689-3

upstream raw materials:

propylamine

oxalyl dichloride

L-threo-2,3-hexodiulosono-1,4-lactone

ethyl 2-(propylamino)-2-oxoacetate

Downstream raw materials:

C₁₈H₁₄BrClF₃N₃O₃

Propyl isocyanate

N,N'-dipropyloxamide

Refernces

• 1、 Zhao, Yu,Mao, Chunhui,Li, Yongqiang,Zhang, Pengxiang,Huang, Zhiqiang,Bi, Fuchun,Huang, Runqiu,Wang, Qingmin. "Synthesis, crystal structure, and insecticidal activity of novel N-alkyloxyoxalyl derivatives of 2-arylpyrrole". experimental part. p. 7326 - 7332. Retrieved 2010/06/11.
• 2、 Wolfs, Ilse,Desseyn, Herman O.. "Hydrogen bond patterns in solid state carboxylic acids. Vibrational behaviour of the catamer pattern as exhibited by the N-alkyloxamic acids". . p. 1521 - 1528. Retrieved 2007/10/03.