p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

Base Information

Chemical Name:p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside
CAS No.:166827-85-6
Molecular Formula:C₆₅H₅₆Cl₃NO₁₉
Molecular Weight:1261.51
Hs Code.:

p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

Synonyms:p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

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Chemical Property of p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

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Technology Process of p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

There total 3 articles about p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: p-Methoxybenzyl 3,6-di-O-benzoyl-2-(benzoyloxyimino)-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-D-arabino-hexopyranoside

: 166827-85-6
p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BH₃*THF, 2.) Na₂CO₃ / 1.) THF, from -10 deg C to RT, 2.5 h, 2.) CH₂Cl₂, RT, overnight

2: pyridine

With pyridine; borane-THF; sodium carbonate;
DOI:10.1246/bcsj.68.1172

Reference yield:

: 98-88-4
benzoyl chloride

: 166827-86-7
C₅₈H₅₂Cl₃NO₁₈

: 166827-85-6
p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

Guidance literature:: With pyridine;
DOI:10.1246/bcsj.68.1172

Reference yield:

: p-Methoxybenzyl 3,6-di-O-benzoyl-2-(benzoyloxyimino)-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-D-arabino-hexopyranoside

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 166827-86-7
C₅₈H₅₂Cl₃NO₁₈

: 166827-85-6
p-methoxybenzyl 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-trichloroethoxycarbonylamino-α-D-glucopyranoside

Guidance literature:: With borane-THF; sodium carbonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, from -10 deg C to RT, 2.5 h, 2.) CH₂Cl₂, RT, overnight;
DOI:10.1246/bcsj.68.1172