4-Phenyl-1,2,3,4-tetrahydroquinoline

Base Information

• Chemical Name: 4-Phenyl-1,2,3,4-tetrahydroquinoline
• CAS No.: 30290-78-9
• Molecular Formula: C₁₅H₁₅N
• Molecular Weight: 209.291
• European Community (EC) Number: 840-870-6
• Nikkaji Number: J3.595.993I

Synonyms:4-phenyl-1,2,3,4-tetrahydroquinoline;30290-78-9;SCHEMBL1045807;AKOS013781954;CS-0162700;E74511;EN300-322737

Chemical Property of 4-Phenyl-1,2,3,4-tetrahydroquinoline

Chemical Property:

• XLogP3: 3.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 209.120449483
• Heavy Atom Count: 16
• Complexity: 220

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CNC2=CC=CC=C2C1C3=CC=CC=C3

Technology Process of 4-Phenyl-1,2,3,4-tetrahydroquinoline

There total 15 articles about 4-Phenyl-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N-[(2E)-3-phenylprop-2-en-1-yl]aniline (92573-86-9) → 4-phenyl-1,2,3,4-tetrahydroquinoline (30290-78-9)

Guidance literature:

With polyphosphoric acid; at 100 ℃; Inert atmosphere;

DOI:10.1080/00397911.2010.493258

Reference yield: 25.0%

N-(3-phenylprop-2-ynyl)benzenamine (121194-51-2) → 4-phenylquinoline (605-03-8) + 4-phenyl-1,2,3,4-tetrahydroquinoline (30290-78-9) + 4‐phenyl‐1,2‐dihydroquinoline

Guidance literature:

With Echavarren's catalyst; In dichloromethane; at 80 ℃; for 0.5h; Sealed tube; Inert atmosphere;

DOI:10.3390/molecules26113366

Reference yield:

4-phenylquinoline (605-03-8) → 4-phenyl-1,2,3,4-tetrahydroquinoline (30290-78-9)

Guidance literature:

With hydrogenchloride; tin; ethanol;

upstream raw materials:

4-phenylquinoline

ethanol

4-phenyl-3,4-dihydro-1H-quinolin-2-one

styrene

Downstream raw materials:

1-methyl-4-phenyl-1,2,3,4-tetrahydroquinoline

phenyl(4-phenyl-3,4-dihydroquinolin-1(2H)-yl)methanone

1-Chloroacetyl-4-phenyl-1,2,3,4-tetrahydroquinoline

4-phenylquinoline

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