N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

Base Information

Chemical Name:N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide
CAS No.:398-11-8
Molecular Formula:C₁₈H₁₁ClF₃NO₂
Molecular Weight:365.739
Hs Code.:

Synonyms:N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

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Chemical Property of N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

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Technology Process of N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

There total 2 articles about N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 92-70-6
3-Hydroxy-2-naphthoic acid

: 121-50-6
3-amino-4-chlorobenzotrifluoride

: 398-11-8
N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

Guidance literature:: With phosphorus trichloride; In chlorobenzene; at 100 - 130 ℃; for 0.75h; Microwave irradiation;
DOI:10.3390/ijms21186583

Reference yield:

: 92-70-6
3-Hydroxy-2-naphthoic acid

: 398-11-8
N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

Guidance literature:: With toluene; trichlorophosphate;

Reference yield:

: 120-35-4
3-amino-4-methoxybenzoic acid phenylamide

: 398-11-8
N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide

: C₃₂H₂₂ClF₃N₄O₄

Guidance literature:: N-[2-chloro-5-(trifluoromethyl)phenyl]-3-hydroxynaphthalene-2-carboxamide; With sodium hydroxide; In methanol; water;

3-amino-4-methoxybenzoic acid phenylamide; With hydrogenchloride; acetic acid; sodium nitrite; In methanol; water; at 5 ℃; Further stages;