4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone

Base Information

• Chemical Name: 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone
• CAS No.: 1357069-65-8
• Molecular Formula: C₃₁H₃₅N₂O₅P
• Molecular Weight: 546.603

Synonyms:4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone

Chemical Property of 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone

Chemical Property:

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Technology Process of 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone

There total 1 articles about 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2,4-di(methoxycarbonyl)-1,5-bis(p-dimethylaminophenyl)penta-1,4-dien-3-one (102989-96-8) + bis(hydroxymethyl)phenylphosphine (3127-08-0) → 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone (1357069-65-8)

Guidance literature:

With pyridine; for 4h; Reflux; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.12.031

Reference yield: 60.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone (1357069-65-8) + isobutylamine (78-81-9) → 1,5-di(carbomethoxy)-6,8-bis(p-dimethylaminophenyl)-3-isobutyl-7-phenyl-3-aza-7-phosphabicyclo[3.3.1]nonan-9-one (1357069-69-2)

Guidance literature:

In methanol; for 24h; Reflux; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.12.031

Reference yield: 45.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-phenyl-2,6-di(carbomethoxy)-3,5-bis(p-dimethylaminophenyl)-4-phosphacyclohexanone (1357069-65-8) + methylamine (74-89-5) → 1,5-di(carbomethoxy)-6,8-bis(p-dimethylaminophenyl)-3-methyl-7-phenyl-3-aza-7-phosphabicyclo[3.3.1]nonan-9-one (1357069-67-0)

Guidance literature:

In ethanol; for 24h; Reflux; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.12.031

upstream raw materials:

2,4-di(methoxycarbonyl)-1,5-bis(p-dimethylaminophenyl)penta-1,4-dien-3-one

bis(hydroxymethyl)phenylphosphine

Downstream raw materials:

1,5-di(carbomethoxy)-6,8-bis(p-dimethylaminophenyl)-3-isobutyl-7-phenyl-3-aza-7-phosphabicyclo[3.3.1]nonan-9-one

1,5-di(carbomethoxy)-6,8-bis(p-dimethylaminophenyl)-3-ethyl-7-phenyl-3-aza-7-phosphabicyclo[3.3.1]nonan-9-one

1,5-di(carbomethoxy)-6,8-bis(p-dimethylaminophenyl)-3-methyl-7-phenyl-3-aza-7-phosphabicyclo[3.3.1]nonan-9-one

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