3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

Base Information

Chemical Name:3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate
CAS No.:1522363-55-8
Molecular Formula:C₁₄H₁₅ClF₃NO₃
Molecular Weight:337.726
Hs Code.:

Synonyms:3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

Chemical Property:

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Technology Process of 3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

There total 3 articles about 3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3282-30-2
pivaloyl chloride

: 1522363-55-8
3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 0 - 20 °C

2: palladium diacetate; dipotassium peroxodisulfate / 20 h / 80 °C / Autoclave

With dipotassium peroxodisulfate; palladium diacetate; triethylamine; In ethyl acetate;
DOI:10.1021/ol403393w

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 1522363-55-8
3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 0 - 20 °C

2: palladium diacetate; dipotassium peroxodisulfate / 20 h / 80 °C / Autoclave

With dipotassium peroxodisulfate; palladium diacetate; triethylamine; In ethyl acetate;
DOI:10.1021/ol403393w

Reference yield:

: 120226-55-3
N-pivaloyl-p-chlorophenylmethylamine

: 76-05-1
trifluoroacetic acid

: 1522363-55-8
3-(4-chlorobenzylamino)-2,2-dimethyl-3-oxopropyl 2,2,2-trifluoroacetate

Guidance literature:: With dipotassium peroxodisulfate; palladium diacetate; at 80 ℃; for 20h; chemoselective reaction; Autoclave;
DOI:10.1021/ol403393w