allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

Base Information

Chemical Name:allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate
CAS No.:1128109-79-4
Molecular Formula:C₂₂H₂₅NO₆S
Molecular Weight:431.51
Hs Code.:

Synonyms:allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

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Technology Process of allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

There total 1 articles about allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 924-44-7
glyoxylic acid ethyl ester

: 941-55-9
4-toluenesulfonyl azide

: 107-18-6
allyl alcohol

: 536-74-3
phenylacetylene

: 1128109-79-4
allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

Guidance literature:: With copper(l) iodide; triethylamine; In tetrahydrofuran; at 25 ℃; for 24h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol900023t

Reference yield: 81.0%

: 1128109-79-4
allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

: 1128110-02-0
N-allyl-N-[3-(ethoxylcarbonyl)-3-hydroxy-2-phenylpropionyl]-(p-tolyl)sulfonamide

Guidance literature:: With bis(benzonitrile)palladium(II) dichloride; In 1,2-dichloro-ethane; at 25 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol900023t

Reference yield: 53.0%

: 1128109-79-4
allyl [3-(ethoxycarbonyl)-3-hydroxy-2-phenyl]-N-(p-toluenesulfonyl)propionimidate

: 1128110-03-1
allyl 3-(ethoxycarbonyl)-3-hydroxy-2-phenylpropionate

Guidance literature:: With water; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 25 ℃; for 33h; Inert atmosphere;
DOI:10.1021/ol900023t