5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Base Information

Chemical Name:5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid
CAS No.:1609699-87-7
Molecular Formula:C₁₅H₁₂BrN₃O₄
Molecular Weight:378.182
Hs Code.:

Synonyms:5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Suppliers and Price of 5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

There total 6 articles about 5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1609699-53-7
methyl 5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoate

: 1609699-87-7
5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Guidance literature:: With water; lithium hydroxide; In methanol; at 80 ℃; for 2h;
DOI:10.1016/j.bmcl.2014.03.100

Reference yield:

: 2150-41-6
methyl 2, 4-dimethoxybenzoate

: 1609699-87-7
5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

2: ethanol / 2 h / Reflux

3: iodobenzene diacetic acid / dichloromethane; methanol / 20 °C

4: lithium hydroxide; water / methanol / 2 h / 80 °C

With iodobenzene diacetic acid; water; titanium tetrachloride; lithium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.03.100

Reference yield:

: 1609699-52-6
methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

: 1609699-87-7
5-(6-bromo-[1,2,4]triazolo[4,3-a]pyridin-3-yl)-2,4-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: iodobenzene diacetic acid / dichloromethane; methanol / 20 °C

2: lithium hydroxide; water / methanol / 2 h / 80 °C

With iodobenzene diacetic acid; water; lithium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.03.100