methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

Base Information

Chemical Name:methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate
CAS No.:1609699-52-6
Molecular Formula:C₁₆H₁₆BrN₃O₄
Molecular Weight:394.225
Hs Code.:

Synonyms:methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

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Chemical Property of methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

Chemical Property:

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Technology Process of methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

There total 3 articles about methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2150-41-6
methyl 2, 4-dimethoxybenzoate

: 1609699-52-6
methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

2: ethanol / 2 h / Reflux

With titanium tetrachloride; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.03.100

Reference yield:

: 91-52-1
2,4 dimethoxybenzoic acid

: 1609699-52-6
methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: dichloromethane / 20 °C

3: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

4: ethanol / 2 h / Reflux

With oxalyl dichloride; titanium tetrachloride; N,N-dimethyl-formamide; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.03.100

Reference yield:

: 39828-35-8
2,4-dimethoxybenzoyl chloride

: 1609699-52-6
methyl 5-((2-(5-bromopyridin-2-yl)hydrazono)methyl)-2,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 20 °C

2: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C

3: ethanol / 2 h / Reflux

With titanium tetrachloride; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.03.100