C₅₂H₄₀BClF₂N₅O₃Re

Base Information

Chemical Name:C₅₂H₄₀BClF₂N₅O₃Re
CAS No.:1421071-29-5
Molecular Formula:C₅₂H₄₀BClF₂N₅O₃Re
Molecular Weight:1053.39
Hs Code.:

C<sub>52</sub>H<sub>40</sub>BClF<sub>2</sub>N<sub>5</sub>O<sub>3</sub>Re

Synonyms:C₅₂H₄₀BClF₂N₅O₃Re

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Chemical Property of C₅₂H₄₀BClF₂N₅O₃Re

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Technology Process of C₅₂H₄₀BClF₂N₅O₃Re

There total 16 articles about C₅₂H₄₀BClF₂N₅O₃Re which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

: 1421071-27-3
C₄₉H₄₀BF₂N₅

: 1421071-29-5
C₅₂H₄₀BClF₂N₅O₃Re

Guidance literature:: With rhenium(I) pentacarbonyl chloride; In toluene; at 110 ℃; for 1h;
DOI:10.1039/c2dt32420b

Reference yield:

: 100-52-7
benzaldehyde

: 1421071-29-5
C₅₂H₄₀BClF₂N₅O₃Re

Guidance literature:: Multi-step reaction with 6 steps

1: trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 12 h / 20 °C

2: triethylamine; boron trifluoride diethyl etherate / dichloromethane / 12 h / 20 °C

3: N-iodo-succinimide / dichloromethane / 1 h / 20 °C

4: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide / tetrahydrofuran; triethylamine

5: triethylamine; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide / 12 h / Inert atmosphere; Reflux

6: rhenium(I) pentacarbonyl chloride / toluene / 1 h / 110 °C

With bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; rhenium(I) pentacarbonyl chloride; boron trifluoride diethyl etherate; triethylamine; triphenylphosphine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; triethylamine; toluene;
DOI:10.1039/c2dt32420b

Reference yield:

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1421071-29-5
C₅₂H₄₀BClF₂N₅O₃Re

Guidance literature:: Multi-step reaction with 6 steps

1: trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 12 h / 20 °C

2: triethylamine; boron trifluoride diethyl etherate / dichloromethane / 12 h / 20 °C

3: N-iodo-succinimide / dichloromethane / 1 h / 20 °C

4: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide / tetrahydrofuran; triethylamine

5: triethylamine; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide / 12 h / Inert atmosphere; Reflux

6: rhenium(I) pentacarbonyl chloride / toluene / 1 h / 110 °C

With bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; rhenium(I) pentacarbonyl chloride; boron trifluoride diethyl etherate; triethylamine; triphenylphosphine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; triethylamine; toluene;
DOI:10.1039/c2dt32420b