methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

Base Information

Chemical Name:methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate
CAS No.:1315336-60-7
Molecular Formula:C₃₄H₅₃N₅O₅Si₂
Molecular Weight:667.996
Hs Code.:

Synonyms:methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

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Chemical Property of methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

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Technology Process of methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

There total 5 articles about methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1315336-59-4
methyl 4-(2-(2-(allyloxy)-4-(bis(2-hydroxyethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1315336-60-7
methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

Guidance literature:: With 1H-imidazole; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja204758c

Reference yield:

: 1315336-57-2
methyl 4-(2-(2-(allyloxy)-4-nitrophenyl)-2H-tetrazol-5-yl)benzoate

: 1315336-60-7
methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; water; iron; acetic acid / Sonication

2: methanol / dichloromethane / 15 h / -78 - 70 °C / pressurized reaction vessel

3: 1H-imidazole; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; methanol; ethanol; water; iron; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja204758c

Reference yield:

: 351188-76-6
(E)-methyl 4-((2-(phenylsulfonyl)hydrazono)methyl)benzoate

: 1315336-60-7
methyl 4-(2-(2-(allyloxy)-4-(bis(2-((tert-butyldimethylsilyl)oxy)ethyl)amino)phenyl)-2H-tetrazol-5-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / -20 °C

2: ethanol; water; iron; acetic acid / Sonication

3: methanol / dichloromethane / 15 h / -78 - 70 °C / pressurized reaction vessel

4: 1H-imidazole; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; methanol; ethanol; water; iron; acetic acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja204758c