potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

Base Information

Chemical Name:potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate
CAS No.:1363407-75-3
Molecular Formula:C₁₄H₁₀BClF₃N₂O₂S*K
Molecular Weight:412.669
Hs Code.:

Synonyms:potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

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Chemical Property of potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

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Technology Process of potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

There total 8 articles about potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: potassium hydrogen difluoride

: 866546-11-4
5-chloro-1-(p-tolylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrolo[2,3-b]pyridine

: 1363407-75-3
potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

Guidance literature:: In methanol; at 20 ℃; for 6h;

Reference yield:

: 1279123-63-5
potassium hydrogenfluoride

: 866546-11-4
5-chloro-1-(p-tolylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrolo[2,3-b]pyridine

: 1363407-75-3
potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

Guidance literature:: In water; acetone; at 20 ℃;

Reference yield:

: 866546-09-0
3-bromo-5-chloro-1 H-pyrrolo[2,3-b]pyridine

: 1363407-75-3
potassium (5-chloro-1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)trifluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.83 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 0 - 25 °C

2.1: potassium acetate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 1,2-dimethoxyethane / 6 h / 86 °C / Inert atmosphere

3.1: water; acetone / 20 °C

With potassium acetate; sodium hydride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone; mineral oil;