4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

Base Information

• Chemical Name: 4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester
• CAS No.: 97801-16-6
• Molecular Formula: C₂₅H₂₉ClN₄O₇
• Molecular Weight: 532.981

Synonyms:4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

Chemical Property of 4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

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Technology Process of 4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

There total 1 articles about 4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

2-(2-azidoethoxy)methyl-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-46-3) + propynoic acid ethyl ester (623-47-2) → 4-(2-Chloro-phenyl)-2-[2-(5-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester (97801-17-7) + 4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester (97801-16-6)

Guidance literature:

In toluene; for 8h; Heating;

DOI:10.1021/jm00168a041

Reference yield: 92.0%

4-(2-Chloro-phenyl)-2-[2-(4-ethoxycarbonyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester (97801-16-6) → 2-[2-(4-Carbamoyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-4-(2-chloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester (97801-20-2)

Guidance literature:

With ammonium hydroxide; In 1,4-dioxane; for 24h; Ambient temperature;

DOI:10.1021/jm00168a041

upstream raw materials:

2-(2-azidoethoxy)methyl-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

propynoic acid ethyl ester

Downstream raw materials:

2-[2-(4-Carbamoyl-[1,2,3]triazol-1-yl)-ethoxymethyl]-4-(2-chloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

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