(((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

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Chemical Name:(((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3
CAS No.:876941-96-7
Molecular Formula:C₆₆H₁₄₄Ge₂Si₁₄
Molecular Weight:1476.25
Hs Code.:

(((CH<sub>3</sub>)3Si)7C<sub>6</sub>H<sub>2</sub>(CH)2C)GeC<sub>6</sub>H<sub>10</sub>GeHC(Si(CH<sub>3</sub>)3)2C<sub>6</sub>H<sub>2</sub>CH(Si(CH<sub>3</sub>)3)2C(Si(CH<sub>3</sub>)3)3

Synonyms:(((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

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Chemical Property of (((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

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Technology Process of (((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

There total 5 articles about (((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 876941-95-6
(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

: 876941-96-7
(((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

Guidance literature:: In benzene-d6; soln. Ge compound in C6D6 was heated at 45 degree.C for 28 h; compound was purified by prep. tlc (hexane);
DOI:10.1021/ja057205y

Reference yield: 44.0%

: 876941-91-2
1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 876941-96-7
(((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

: 876941-97-8
(((CH₃)3Si)7C₆H₂(CH)2C)2(GeC₆H₁₀)2

Guidance literature:: In hexane; under Ar atm. to soln. Ge compound in hexane was added soln. excess 2,3-dimethyl-1,3-butadiene in hexane at room temp., mixt. was stirred for 24h; soln. was evapd. in vac., residue was purified by GPLC and WCC; elem. anal.;
DOI:10.1021/ja057205y

Reference yield:

: 857444-41-8
(E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 876941-96-7
(((CH₃)3Si)7C₆H₂(CH)2C)GeC₆H₁₀GeHC(Si(CH₃)3)2C₆H₂CH(Si(CH₃)3)2C(Si(CH₃)3)3

Guidance literature:: Multi-step reaction with 3 steps

1: KC₈ / benzene

2: hexane

3: benzene-d6

With KC₈; In hexane; benzene-d6; benzene;
DOI:10.1021/ja057205y