1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

Base Information

Chemical Name:1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline
CAS No.:90065-60-4
Molecular Formula:C₁₉H₂₂N₂O
Molecular Weight:294.396
Hs Code.:

Synonyms:1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

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Chemical Property of 1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

Chemical Property:

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Technology Process of 1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

There total 4 articles about 1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Dimethyl-(4-phenyl-3,4-dihydro-isoquinolin-1-ylmethyl)-amine

: 90065-60-4
1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / methanol / 16 h / 2068.6 Torr

2: 12.6 g / toluene / Heating

With hydrogen; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jm00374a011

Reference yield:

: 90065-24-0
N-(chloroacetyl)-2,2-diphenylethylamine

: 90065-60-4
1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 88.1 g / P₂O₅ / xylene / 2 h / Heating

2: methanol / 4 h / 0 - 20 °C

3: H₂ / 5percent Pd/C / methanol / 16 h / 2068.6 Torr

4: 12.6 g / toluene / Heating

With hydrogen; phosphorus pentoxide; palladium on activated charcoal; In methanol; toluene; xylene;
DOI:10.1021/jm00374a011

Reference yield:

: 91123-65-8
1-(chloromethyl)-3,4-dihydro-4-phenylisoquinoline hydrochloride

: 90065-60-4
1,2,3,4-tetrahydro-2-formyl-1-<(dimethylamino)methyl>-4-phenylisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 4 h / 0 - 20 °C

2: H₂ / 5percent Pd/C / methanol / 16 h / 2068.6 Torr

3: 12.6 g / toluene / Heating

With hydrogen; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jm00374a011