N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester

Base Information

• Chemical Name: N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester
• CAS No.: 857078-06-9
• Molecular Formula: C₂₇H₂₆N₂O₆S
• Molecular Weight: 506.579

Synonyms:N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester

Chemical Property of N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester

Chemical Property:

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Technology Process of N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester

There total 5 articles about N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-4-nitrobenzene (92-93-3) → N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester (857078-06-9)

Guidance literature:

Multi-step reaction with 5 steps

1: ClSO₃H / CHCl₃ / 60 °C

2: SOCl₂ / Heating

3: NaHCO₃ / CH₂Cl₂

4: SnCl₂ / dimethylformamide

5: i-Pr₂EtN / CH₂Cl₂

With chlorosulfonic acid; thionyl chloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; In dichloromethane; chloroform; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2005.06.019

Reference yield:

4'-nitrobiphenyl-4-sulfonyl chloride (20443-75-8) → N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester (857078-06-9)

Guidance literature:

Multi-step reaction with 3 steps

1: NaHCO₃ / CH₂Cl₂

2: SnCl₂ / dimethylformamide

3: i-Pr₂EtN / CH₂Cl₂

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2005.06.019

Reference yield:

4-nitrobiphenylsulfonic acid (91493-72-0) → N-({4'-[(1-benzofuran-2-ylcarbonyl)amino]-1,1'-biphenyl-4-yl}sulfonyl)glycine t-butyl ester (857078-06-9)

Guidance literature:

Multi-step reaction with 4 steps

1: SOCl₂ / Heating

2: NaHCO₃ / CH₂Cl₂

3: SnCl₂ / dimethylformamide

4: i-Pr₂EtN / CH₂Cl₂

With thionyl chloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2005.06.019

upstream raw materials:

2-benzofuroyl chloride

(S)-2-(4'-amino-biphenyl-4-sulfonylamino)-3-methyl-butyric acid tert-butyl ester

1-phenyl-4-nitrobenzene

4'-nitrobiphenyl-4-sulfonyl chloride

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