(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

Base Information

Chemical Name:(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol
CAS No.:120410-08-4
Molecular Formula:C₂₇H₃₈O₂
Molecular Weight:394.598
Hs Code.:

Synonyms:(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

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Technology Process of (R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

There total 1 articles about (R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 93178-06-4
(3S,8R)-9-benzyloxy-7-chloroirid-1-ene

: 3865-09-6,38231-11-7,83945-83-9,93221-52-4
(R)-2-methyl-5-(prop-1-en-2-yl)cyclopent-1-ene-1-carbaldehyde

: 120410-19-7
(S)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

: 120410-08-4
(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

Guidance literature:: With chromium dichloride; In tetrahydrofuran; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/c39880000354

Reference yield: 100.0%

: 75-77-4
chloro-trimethyl-silane

: 120410-08-4
(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

: 120410-15-3
[(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methoxy]-trimethyl-silane

Guidance literature:: In pyridine; at 20 ℃; for 15h;

Reference yield:

: 120410-08-4
(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-((R)-5-isopropenyl-2-methyl-cyclopent-1-enyl)-methanol

: 120354-76-9
(R)-2-((R)-2-{(R)-[(1R,3S)-3-((R)-2-Benzyloxy-1-methyl-ethyl)-1-methyl-2-methylene-cyclopentyl]-hydroxy-methyl}-3-methyl-cyclopent-2-enyl)-propionaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: 2CHCH(Me)>2BH, H₂O₂/OH^(1-)

3: pyridinium chlorochromate / CH₂Cl₂

4: 90 percent / KF-Florisil / methanol

5: 100 percent / pyridinium toluene-p-sulphonate / tetrahydrofuran; H₂O

With pyridine; potassium fluoride; florisil; hydroxide; dihydrogen peroxide; pyridinium p-toluenesulfonate; bis-(1,2-dimethylpropyl)borane; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c39880000354