trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester
CAS No.:1206181-57-8
Molecular Formula:C₁₄H₉F₃N₂O₅S₂
Molecular Weight:406.363
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

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Technology Process of trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

There total 1 articles about trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 677302-48-6
1-benzenesulfonyl-1,4-dihydro-5H-pyrrolo[3,2-b]pyridin-5-one

: 1206181-57-8
trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.416667h;
DOI:10.1016/j.tet.2009.11.040

Reference yield: 99.0%

: 60-35-5
acetamide

: 1206181-57-8
trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

: 1206181-87-4
N-(1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl)acetamide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; for 1.5h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.040

Reference yield: 97.0%

: 1206181-57-8
trifluoromethanesulfonic acid 1-benzenesulfonyl-1H-pyrrolo[3,2-b]pyridin-5-yl ester

: 1692-15-5
4-pyridylboronic acid

: 1206181-63-6
1-benzenesulfonyl-5-pyridin-4-yl-1H-pyrrolo[3,2-b]pyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2009.11.040