Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

aceroside IV perbenzoate

Base Information Edit
  • Chemical Name:aceroside IV perbenzoate
  • CAS No.:197382-99-3
  • Molecular Formula:C53H46O12
  • Molecular Weight:874.941
  • Hs Code.:
  • Mol file:197382-99-3.mol
aceroside IV perbenzoate

Synonyms:aceroside IV perbenzoate

Suppliers and Price of aceroside IV perbenzoate
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 0 raw suppliers
Chemical Property of aceroside IV perbenzoate Edit
Chemical Property:
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of aceroside IV perbenzoate

There total 15 articles about aceroside IV perbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/jo981844s
Guidance literature:
Multi-step reaction with 13 steps
1.1: 96 percent / K2CO3 / dimethylformamide / 24 h / 60 °C
2.1: 97 percent / LAH / tetrahydrofuran / 45 h / 0 °C
3.1: pyridine / 20 °C
4.1: 1.31 g / NaI / acetone / Heating
5.1: LDA / tetrahydrofuran / 0.33 h / 0 °C
5.2: 80 percent / tetrahydrofuran / 0.33 h / 0 °C
6.1: NaH / tetrahydrofuran / 0.33 h / 0 °C
6.2: 76 percent / tetrahydrofuran / 1 h / 0 °C
7.1: BCl3 / CH2Cl2 / 1 h / 0 °C
8.1: 1.25 g / aq. HCl / 24 h / Heating
9.1: 95 percent / CsF / dimethylformamide / 5 h / 20 °C
10.1: 100 percent / H2 / Pd/C / methanol / 1 h
11.1: 90 percent / tert-butyl nitrite / dimethylformamide / 1 h / 50 °C
12.1: 88 percent / AlCl3 / CH2Cl2 / 18 h / Heating
13.1: 93 percent / aq. NaOH; tetrabutylammonium bromide / CH2Cl2 / 5 h / 20 °C
With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; tert.-butylnitrite; tetrabutylammomium bromide; hydrogen; boron trichloride; sodium hydride; potassium carbonate; cesium fluoride; sodium iodide; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; 1.1: Etherification / 2.1: Reduction / 3.1: Tosylation / 4.1: Substitution / 5.1: Metallation / 5.2: Alkylation / 6.1: Metallation / 6.2: Alkylation / 7.1: dealkylation / 8.1: Decarboxylation / 9.1: Cyclization / 10.1: Hydrogenolysis / 11.1: Deamination / 12.1: demethylation / 13.1: glycosidation;
DOI:10.1021/jo981844s
Guidance literature:
Multi-step reaction with 8 steps
1.1: NaH / tetrahydrofuran / 0.33 h / 0 °C
1.2: 76 percent / tetrahydrofuran / 1 h / 0 °C
2.1: BCl3 / CH2Cl2 / 1 h / 0 °C
3.1: 1.25 g / aq. HCl / 24 h / Heating
4.1: 95 percent / CsF / dimethylformamide / 5 h / 20 °C
5.1: 100 percent / H2 / Pd/C / methanol / 1 h
6.1: 90 percent / tert-butyl nitrite / dimethylformamide / 1 h / 50 °C
7.1: 88 percent / AlCl3 / CH2Cl2 / 18 h / Heating
8.1: 93 percent / aq. NaOH; tetrabutylammonium bromide / CH2Cl2 / 5 h / 20 °C
With hydrogenchloride; sodium hydroxide; aluminium trichloride; tert.-butylnitrite; tetrabutylammomium bromide; hydrogen; boron trichloride; sodium hydride; cesium fluoride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 1.1: Metallation / 1.2: Alkylation / 2.1: dealkylation / 3.1: Decarboxylation / 4.1: Cyclization / 5.1: Hydrogenolysis / 6.1: Deamination / 7.1: demethylation / 8.1: glycosidation;
DOI:10.1021/jo981844s
Post RFQ for Price