Cyclohexyl-sulfamic acid cyclohexyl ester

Base Information

• Chemical Name: Cyclohexyl-sulfamic acid cyclohexyl ester
• CAS No.: 82962-26-3
• Molecular Formula: C₁₂H₂₃NO₃S
• Molecular Weight: 261.386
• Mol file: 82962-26-3.mol

Synonyms:Cyclohexyl-sulfamic acid cyclohexyl ester

Chemical Property of Cyclohexyl-sulfamic acid cyclohexyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Cyclohexyl-sulfamic acid cyclohexyl ester

There total 1 articles about Cyclohexyl-sulfamic acid cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

cyclohexylsulfamoyl chloride (10314-35-9) + cyclohexanol (108-93-0) → Cyclohexyl-sulfamic acid cyclohexyl ester (82962-26-3)

Guidance literature:

With sodium carbonate; tetrabutylammomium bromide; In benzene; for 1h; Ambient temperature;

DOI:10.1055/s-1985-31390

Reference yield: 87.0%

Cyclohexyl-sulfamic acid cyclohexyl ester (82962-26-3) + allyl bromide (106-95-6) → Allyl-cyclohexyl-sulfamic acid cyclohexyl ester (104254-98-0)

Guidance literature:

With calcium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; at 20 ℃; for 23h;

DOI:10.1055/s-1985-31390

Reference yield: 75.0%

Cyclohexyl-sulfamic acid cyclohexyl ester (82962-26-3) + methyl iodide (74-88-4) → Cyclohexyl-methyl-sulfamic acid cyclohexyl ester (104254-96-8)

Guidance literature:

With sodium hydroxide; potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride; at 20 ℃; for 0.25h;

DOI:10.1055/s-1985-31390

upstream raw materials:

cyclohexylsulfamoyl chloride

cyclohexanol

Downstream raw materials:

Cyclohexyl-(2,4-dinitro-phenyl)-sulfamic acid cyclohexyl ester

Allyl-cyclohexyl-sulfamic acid cyclohexyl ester

Cyclohexyl-methyl-sulfamic acid cyclohexyl ester