salicylaldehyde diphenyl dithioacetal

Base Information

• Chemical Name: salicylaldehyde diphenyl dithioacetal
• CAS No.: 18268-10-5
• Molecular Formula: C₁₉H₁₆OS₂
• Molecular Weight: 324.467
• Mol file: 18268-10-5.mol

Synonyms:salicylaldehyde diphenyl dithioacetal

Chemical Property of salicylaldehyde diphenyl dithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of salicylaldehyde diphenyl dithioacetal

There total 6 articles about salicylaldehyde diphenyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-methyl-benzyl alcohol (89-95-2) + thiophenol (108-98-5) → salicylaldehyde diphenyl dithioacetal (18268-10-5)

Guidance literature:

With boron trifluoride diethyl etherate; In acetic acid; toluene;

DOI:10.1016/S0040-4039(00)00753-X

Reference yield: 80.0%

salicylaldehyde (90-02-8) + thiophenol (108-98-5) → diphenyldisulfane (882-33-7) + salicylaldehyde diphenyl dithioacetal (18268-10-5)

Guidance literature:

With graphene oxide; In neat (no solvent); at 60 ℃; for 10h; chemoselective reaction; Green chemistry;

DOI:10.1016/j.tetlet.2014.10.043

Reference yield: 50.0%

salicylaldehyde (90-02-8) + dimedone (126-81-8) + thiophenol (108-98-5) → 2,3,4,9-tetrahydro-9-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-3,3-dimethyl-1H-xanthen-1-one (19744-87-7) + 3,3-dimethyl-9-(phenylthio)-2,3,4,9-tetrahydro-1H-xanthen-1-one (1397291-12-1) + salicylaldehyde diphenyl dithioacetal (18268-10-5)

Guidance literature:

With sarcosine; In ethanol; at 80 ℃; for 15h; Reagent/catalyst; Solvent;

DOI:10.1039/c2gc35668f

upstream raw materials:

2-methyl-benzyl alcohol

thiophenol

salicylaldehyde

dimedone

Downstream raw materials:

[2-(bis-phenylsulfanyl-methyl)-phenoxy]-tert-butyl-dimethyl-silane

1-(Bis-phenylsulfanyl-methyl)-2-(3-methyl-but-3-enyloxy)-benzene

2,3-dihydro-1-benzoxep-4-ene

salicylaldehyde